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  • Article title
  • Abstract
  • Keywords
  • Introduction
  • Experimental
    • Materials and reagents
    • Instruments and equipment
    • Preparation of solutions
      • Preparation of diluent
      • Preparation of standard solution
      • Preparation of sample solution
      • Preparation of sample spiked solution
  • Instrumentation
    • Method development
      • Diluent for sample and standard preparation
      • Chromatographic and headspace parameters conditions
    • Method validation (ICH 2005)
      • Specificity
      • System precision
      • Detection limit (LOD), Quantitation limit (LOQ)
      • Method precision
      • Linearity and range
      • Accuracy
      • Solution stability
  • Conclusion
  • Acknowledgment
  • References
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